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If you are referring to the period of colonization and colonialism, certainly one of the first was the United States of America, which declared its independence from England in 1776; the Americans fought and won the Revolutionary War (1775-1781). Another early country to declare independence was Haiti, which gained its freedom from France in 1804.
Egypt (1922) was the first African nation to become independent from a European nation, but it was not a colony (it was a protectorate). The first colony to become independent was Italian Libya in 1951.
Haiti.
The first war of independence started on 1857.
Missionaries